Sintesis Timah (II) Sulfat (SnSO4) Menggunakan Metode Elektrolisis dengan Parameter Tegangan, Konsentrasi, Waktu dan Jarak Elektroda

Abstract

Tin (II) Sulfate (SnSO4) a tin-derived product that has a wide range of physical and chemical functions. The synthesis of tin (II) sulfate (SnSO4) has been carried out using the parameters of voltage, electrolyte concentration, electrolysis time and electrode spacing with the aim of producing SnSO4 precipitates and knowing the optimum parameters of the synthesis process using the electrolysis method. The samples were analyzed using X-Ray Diffraction (XRD) and Fourier Transform InfraRed (FT-IR), Differential Thermal Analysis (DTA), and Iodine test. The results concluded that SnSO4 was not fully optimized due to the presence of impurities due to the formation of Sn4+ during the electrolysis process. Based on the results of the analysis using the Taguchi Method, the most influential parameter because it has a small signal to noise ratio (S/N Ratio) is the electrode spacing.