Sintesis Kompleks Paladium (II) Klorida dengan Ligan BIS (2,5-Dimetoksifenil) Fenilfosfina

Abstract

Bis-(2,5-dimethoxyphenyl) phenylphosphine (BDFF) ligand can be synthesized from 1,4-dimethoxybenzene and dichlorophenylphosphine via lithiation using n-BuLi/TMEDA. The ligand was reacted with % equivalent [Pd(MeCN).Ck,] to form mononuclear, [PdClaBDFF).] complex. The structure of

the ligand and complex were confirmed by FT-IR, ‘H and *'P{’H}-NMR.

spectroscopies.